Determination of multi-pesticide residues in honey with a modified QuEChERS procedure followed by LC-MS/MS and GC-MS/MS
Beste Oymen, S. Aşır, Deniz Türkmen, A. Deni̇zli̇
- Yazarlar
- Beste Oymen, S. Aşır, Deniz Türkmen, A. Deni̇zli̇
- Yayın
- Journal of Apicultural Research 2022
- DOI
- 10.1080/00218839.2021.2017540
- Atıflar
- 23
Özet
This paper presents a modified QuEChERS method to determine 346 pesticide residues in honey by LC/MS-MS and GC/MS-MS. Acetate buffered acetonitrile extraction followed by dispersive SPE clean-up with C18-E, PSA and MgSO4 sorbents were used for sample preparation. This method was validated according to the European Union SANTE/2019/12682 guidelines. Acceptable values were obtained for the linearity, the limit of detection (0.001–0.003 mg/kg), limit of quantification (0.002–0.008 mg/kg), trueness (for the four tested levels, the recovery assays values were between 76 and 112%), precision (RSD ≤20.0%) and measurement uncertainty tests (
Bu makaleye atıf yapın
Beste Oymen, S. Aşır, Deniz Türkmen, A. Deni̇zli̇ (2022). Determination of multi-pesticide residues in honey with a modified QuEChERS procedure followed by LC-MS/MS and GC-MS/MS. Journal of Apicultural Research. https://doi.org/10.1080/00218839.2021.2017540
BibTeX
@article{beste2022,
title = {Determination of multi-pesticide residues in honey with a modified QuEChERS procedure followed by LC-MS/MS and GC-MS/MS},
author = {Beste Oymen and S. Aşır and Deniz Türkmen and A. Deni̇zli̇},
journal = {Journal of Apicultural Research},
doi = {10.1080/00218839.2021.2017540},
year = {2022}
}